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no problems here with 24/96 files... what version of FLAC are you using?
Possibly is the wav header messed up? Maybe FLAC can't determine the sampling rate, #of bits, # of channels .
i thought it was cd wave editor, not wavelab, that gave you the "save in alternate 24 bit format" option...that's where i've always had problems with 24bit files and FLAC - the way cd wave editor saves them if you don't check that box.